| GC-MS/MS, Triple Quadrupole with EI, CI, NCI, NIST Library, and Method Package |
| Features The Gas Chromatograph triple quadruple Mass Spectrophotometer system is fully computer controlled and run under Windows Operating system.All gas flow including septum purge should be automatically controlled by flow controller from software.The one touch injection maintenance button prepares GC for injection unit maintenance. System must be capable of different column oven cooling rate fast, middle, slow and customized to protect column.System should have touch screen user friendly interface. |
| Technical Specifications: |
| Brand | : Shimadzu Corporation, Japan |
| Model | : GCMS-TQ8050NX |
| Must be possible to install 4 detectors and 3 sample injection system simultaneously and individually temperature controlled on the GC and software. |
| Extensive self-diagnostic functions which must be supported details diagnosis of electrical system like DC voltage, gas pressure and sensors errors. |
| GC itself must have a 7 in colour touch screen with 480×800 dot format. |
| Tools free technology for column installation |
| Should have automatically compensates for variations in atmospheric pressure and temperature. |
| Should have 3 different types of flow control modes: Constant Pressure, constant column flow and constant linear velocity for better peak separation and resolution. |
| There must be an oven door sensor that will automatically shut off all temperature when door is open or not closed properly. |
| Retention time Repeatability: <0.0008 min |
| Peak area repeatability: < 1% RSD |
| Column Oven | Oven Volume 13.7L or more |
| Should be fits up to two 100m X 0.53mm ID capillary column. |
| Operating temperature range: ambient + 2°C to 450° |
| Oven must have temperature program steps up to 32 (cooling program must be possible). |
| Maximum achievable temperature ramp rate must be 120°C/min. |
| Programmed rate setting range -250 to 250 º C/min |
| Maximum run time: 9999.99 minutes |
| Oven cools down from 450°C to 50°C must take not more than 3.4 mins |
| Ambient Rejection: < 0.01°C per 1°C |
| Temperature Setpoint resolution 0.1°C |
| Temperature Accuracy: set value (K) ±1% |
| Temperature Deviation :<2 º C |
| Split/Splitless Injector | Must have Split, Splitless, High pressure injection mode |
| Must be suitable for all capillary columns, 50 µm to 530 µm id. |
| Must have gas saver mode to reduces gas consumption |
| Split ratio up to 9999.9:1. |
| Maximum operating temperature up to 450°C. |
| All Gas Flow must be controlled by Electronic flow controller |
| Pressure Range 0 to 1035 Kpa. ( 0 to 150 psi) |
| 7 pressure program ramps possible |
| Pressure set point resolution: 0.1 Kpa ( 0.001 Psi) |
| Pressure sensor accuracy :< ±2.0 % Full scale |
| Pressure Drift: < ±0.68 Kpa/6 months. |
| Maximum gas flow up to 1300 mL/min |
| Flow setpoint resolution 0.1mL/min |
| Flow ramps 7 |
| Flow sensor accuracy: < ± 5% |
| Triple Quadrupole Mass Spectrometer:The collision gas should be Argon. The quadrupoles must be made up of metal rods with pre-rod.The Collision cell must be high efficiency collision cell “UFsweeper” for efficient ion acceleration and removing ion rapidly to minimize cross-talk.The collision energy should be 0 to 60V or higher.The icon path shall be off axis to reduce neutral noise before reaching the detector.The mass spectrometer must have Electron Ionization (EI), Chemical Ionization (CI) & Negative Chemical Ionization (NCI) modes.The mass spectrometer must be equipped with an ultra-high sensitivity ion source that has a shield blocks out radiant heat generated from the filament to ensure the ion source box temperature remains uniform. Since this prevents any active spots within the ion source, it provides higher sensitivity for analysis.Mass range: 10 to 1090 amu Mass resolution: 0.4 to 3.0 u (FWHM) The scanning speed capability up to 20,000 amu/sec.It have scan cycle of up to 333 scan/sec in order to obtain highly precise data for fast GCMS.The collision cell must be capable performing MRM analysis with the shortest Dwell time of <0.5 msec.MRM transition speed must be 800 MRM transitions/sec.The mass spectrometer should have a stability of ±0.1u over 48 hours.The ion source and interface must be independently heated over a user-selectable temperature range.Ion Source: 140 to 350°CInterface: 50 to 350°CElectron energy setting between 10 to 200 eVEmission current should be 5 to 250µA.The ion source must be accessible from the front for ease of maintenance without the need to remove the top cover.Detector must be a Secondary electron multiplier with overdrive lens and conversion dynode.The dynamic range should be 8 x 106. It must have MS acquisition modes: Q1 Scan, Q3 Scan, Product Ion scan, Precursor Ion scan, Neutral Loss Scan, Q1 SIM, Q3 SIM, MRM, Scan/SIM and Scan/MRM FASSTAutomated MRM optimization with automated optimization of collision energy (CE) and automated method creation for the MRM measurement must be available. The mass spectrometer should employ a unique over-drive lens to minimize random noise enhancing the Signal-to-Noise.The EI MRM IDL [Instrument Detection Limit] must be below 0.5 fg OFN (Octafuoronaphthalene) statistically derived at 99% confidence level from the area precision of eight consecutive spitless injections of 1 ul, 2 fg/ul OFN Standard for transition of 272 →222.The vacuum system should be maintained by a Differential Pumped Turbo Molecular Pump with a pumping capacity of 360 L/sec, Fore pump: Oil Rotary Pump: 30L/min and Column Flow: 10mL/min.The vacuum system must be able to accommodate flow rates up to 10.0 mL/min of helium enabling highly effective evacuation speeds and increases allowable column flow rates. Must have built in Automatic Adjustment of Retention Time (AART) capability to adjust the retention times of target compounds even for simultaneous MRM analysis of multiple components. Must have eco-friendly feature which reducing energy consumption during standby operation.The mass spectrometer must have Twin-Line capability to install two narrow-bore capillary columns into the MS simultaneously in order to eliminate the need to swap columns when switching applications.Optimized MRM method/database for pesticides and environmental analysis must be available. |
| Sensitivity: |
| EI scan sensitivity: | Signal-to-noise (S/N) ≥ 2000 at m/z 272 for 1 pg. octafluoronapthalene (OFN) in EI scan |
| EI MRM sensitivity: | Signal-to-noise (S/N) ≥ 40, 000 for the transition from m/z 272 to m/z 222 for 100fg octafluoronapthalene (OFN) in EI MRM |
| CI MRM sensitivity: | Signal-to-noise (S/N) ≥ 5000 for the transition from m/z 193 to m/z 110 for 1 pg. benzophenone d10 in CI MRM |
| NCI SIM sensitivity: | Signal-to-noise (S/N) ≥ 10000 at m/z 272 for 100fg octafluoronapthalene (OFN) in NCI sensitivity |
| Auto Injector: | Peak area repeatability: < 0.3 % RSD or betterSample discrimination: < 10 % or betterSample injection linearity: < 5 % or betterSample carryover: < 5 ppm or better1.5 mL sample vial capacity: 30 or more |
| Software System: | The system software should be true 32-bit/64-bit application software based on user friendly Microsoft Windows operating environment. System start-stop should be fully automated and controlled via the software.Automated MRM optimization with automated optimization of collision energy (CE) and automated method creation for the MRM measurement must be available.Reporting format functions must be flexible and be based on users’ design.This software must be fully GLP/GMP compliance. Strong security function, validation function, and audit trail function for data traceability must be built-in as a standard.The library search software is provided as standard. The library search mode should be either by similarity search or index search. |
| Accessories | a) GC-MS startup kitb) Consumable & Installation Kitsc) 20 mL Headspace crimp vial with Cap & Septa- 200 pcsd) Crimper and Decapper for 20 mL vials- 01 of eache) GC Vial (1.5 mL) with Cap and Septa- 1000 pcsf) Micro-insert for ND9 wide opening vial- 500 pcsg) Hydrophobic syringe filter (0.22 and 0.45µm) – 500 pcs of each h) Vespel ferrule (0.4 and 0.5 OD)- 50 pcs of eachi) Sky liner/Topaz Liner, splitless (5pcs/pkt)- 03 pktj) Microliter syringe, 10ul, fixed needle-Qty:03k) NIST mass spectrum library (latest version)l) MS columns- 5 Nos. m) Smart Metabolites Databasen) GC/MS Residual Pesticides Database(English) o) One set of 1st Filling of Helium, Ar, CH4 Gas Cylinder with Regulatorsp) Carrier Gas supply pipes (02pcs)q) An installation Table with cabinet and rack. |
| Computer | Brand Computer- 1No.Processor- Intel Core i9-11900, RAM: 16 GB, SSD: 1TB, Original Windows latest version with original MS office, Optical Drive: DVD-R/W, Monitor: 27 Inch LED. |
| Online UPS | 10 KVA On-line UPS with built-in Stabilizer, 60min back up at full load- 01 No. |
| Printer | HP/Canon Laser Printer with auto-Duplex- 1No. |
| Country of Origin | Japan. |
| Make and assembly | Japan. |
| Certification- Country of Origin | Yes |
| Manufacturer Authorization Letter | Yes (On Manufacturer’s letterhead pad) |
| Manufacturer Warranty and guaranty | Yes (On Manufacturer’s letterhead pad) |
| Standard Warranty and guaranty | One Year |
| Extended Service Warranty | Five years (including warranty period) |
| Training | 5 days training on maintenance, trouble shooting, operation, and application of equipment must be provided by manuufacturer trained engineer after installation and commissioning and 3-days after 3-months of 1st schedule training at user site. We will train up the appointed scientists/experts/technician until ready for operation. |
| Advance Foreign Training | Advance foreign training on Operation and application will be provided by us in the manufacturer country or manufacturer permitted country’s Laboratory for 5 (five) working days. We will bear all costs like transportation and accommodation with daily allowance as required as need in standard rules and regulation. |
| Packing list | Packing list from manufacturer will be provided with system |
| Catalog | Manufacturer catalogue submitted in English |
| Remarks (any) | N/A |
| Price | Included |
